I did DIY CO2 on a 240 gallon tank, heavily planted. I typically ran two 2liter bottles of sugar and yeast. What made the biggest difference was the reactor you use. I had a bubble track, which extended the time the bubbles were in contact, and worked ok. What made the biggest difference was my DIY reactor, which was PVC pipe capped at both ends, weighted at one end, and holes drilled in the pipe for the co2 line, pump inlet, and water outlet. The pump was on the light timer circuit. The PVC captures the co2, and the pump pushed water into the pipe, creating more surface area and contact time. This worked great for increasing the co2 levels.
For a 75 gallon , sugar and yeast can work; for larger tanks it does become a bit tiresome to be changing the sugar solution weekly, and pressurized co2 probably becomes more cost effective in the long run.