Technical speaking, no I'm not using "pure" laboratory grade ammonia. I'm using cleaning grade ammonia with only 1 ingredient: Ammonium Hydroxide, which of course is just an aqueous solution of ammonia. There is no coloring, perfumes/scents, or sulfactants/soaps that are listed on the bottle. I understand it probably has negligible amounts of contaminants; this is the same gallon jug I have used on easily 20 tanks in the past year, and I have not had a problem yet. I am very confident that the ammonia I am using is not the problem.
As far as numbers go; I have not documented the process day by day as there really isn't much to it.
I add enough ammonia to get an initial reading of about 2-3 PPM (which I have found to provide faster cycling than higher concentrations). After about a week I start to test the ammonia level and add more ammonia as needed to get the concentration back to 2-3 PPM, once per day, as close as 24 hours after the last ammonia addition as possible. This involves a test to get the starting concentration in the tank, and a test (sometimes more) after the additional ammonia is added. On this particular brand of ammonia, it takes about 3 capfuls to jump the tank PPM up 2 PPM.
I usually do a test for nitrite every couple of days during the first part of the cycle to determine if the ammonia is getting broken down. My kit tested positive for nitrite about a week into the cycle. I did not pay attention to the value at the time, as it wasn't important.
Being that I used pre seeded media, I started to see a .5 to 1 PPM drop per day after a week. This slowly increased (I would guess .25 per 2 1/2 days??) until a test showed no ammonia in the tank. As witnessed before, ammonia breakdown seems to happen at an increasing pace, as opposed to nitrite which seems to plateau and then drop off suddenly over a day or two. At this point, I tested for nitrite, expected to see it in the tank, but found that this part of the cycle had also completed.
My test for nitrate at this point showed medium red on the API drop test; I would guess in the 80 PPM range.
The next day, the test for ammonia showed an increase in ammonia, even through I had not introduced any to the tank since the last test. The reading was between 1-2 PPM.
I have continued by cycling procedure, bringing the concentration up to 2-3 PPM per day, and 24 hours later I still see .75 to 1 PPM left over in the tank. Nitrites have been at 0 since I started testing for them daily.
I just tested the water, which is about 25 hours since the test yesterday. Here are my readings:
ammonia: .75 (between .5 and 1 ppm)
nitrite: 0 ppm
nitrate: between 40-80 PPM
This means that roughly half of the ammonia added is getting broken down per day. Why not the other half? This has been going on for weeks...I can't make heads or tails of it.